Обработка экспериментальных данных

. 4.12. & , 5 & , & &/ 0. ..

. 4.13. 5 4 -44 . &/ 5 , & .

51

-, . &/ 0 0 . 9 , &/ / . Lack-of-Fit Test.

& , 5 & & 6 , , , .07 0 / . 3 0 / ,6 Pane Options. ! 0 7 .

69 6 / . Include Lack-of-Fit Test.

. 4.14. 4 , 1 &.

! 6&/, & , 5 & 6 6 & 0

0, , &6+ 0 1 (Lack-of-fit, . 4.12). &/ 6

+ p-Value, 0+ & 1 &/7 + . 0.05, , &6+ . &/ 5 , & & ,

&.

6&/ 0 , 5 &, , 0 38, +

+ 01 +& . 3 + + .0 -44 0, , 9 3 & . 0 5 4 . -44

. &/ 5 , & ( . 4.13).

. -, , 5 & & & & & + 4, 01 &8 &

. . &/. & 5& -6 & / . 9 0 / , . 8/3 5 4 , 1 &.

& -5 & 6 0 / & 5 5 4 + 1 46 0 / ,6 first Response Plot, 6&/ + 5 6 &

52

638 5 4 + ( . 4.14). 2 1. 0 5 4 . 1 &. 7 (, & &/) + 0.83 ( ), 0.85 ( ). . 9 & / . . &/ &8 & 9 , & 1 0.80

0.87 , 0.70 0.96 , .

+ 0. 6&/ . , 5 -, . &

& + . / :

T = -38,2387 + 115,029 A - 3,89637 B - 76,6666 A2 + 16,0 A B - 5,70005 B2

4.3. 0# " 0$ ! # % & 2 ! ! !# 3 % -.

/ & . ., + ., 0,

01 . /, 6.. &9 0 / 6. , ., & 1 . , . / 6 4 6 5 ,6 7, 8 5

5 4 6, 6.. & 1 . &9 0 /

100%. 0 + , . . + / + +

, 8, 4 . + 1 . + , .07&.

8 . , ., , . 8/3 5 . 56 0 / , & 0 , , ., & 3 65 &/ 0 5 ..0 (5 ..0

65 &/). & , , & 9 /, + . . /,

3 ., A, B, C (& 3.3), &3 . / 1 ., . 9 0 / , & + . 65 &/, , & . . , . 0..

6.. & 9 . 1, + + .,

9 . . 56 , / , ,. & -

0 5 4, +, + + 63 65 &/

3-1 . . ,. ! 7, 638 .6

4 6 , & + 63 . /, 863 &/

., 0. + 638 7 ., 0

1 (100% & &3 65 & + . 7 &0)

0 & 1 65 1 .,. , , , & 9

638 7, + ., 0 0, & 65 1 ., 0.5 (50% &).

53

0+ , &/ 63 , 01 ,& -, . & .. 3 , 1 & 7 1

65 &/ 1 . $5 - ,& 0 & 3

, & &/ 0 6 +.

, . - & 9 5 4 & ., 0 . & 63 . 8 0 +, 9

1 ..

!&6+ , &/ - + ,&

63 . , . + 01 . (, ., 1 0 0; 0 1 0; 0 0 1), , . . 0. , , , ., .

&.

!, . 9 , . 6 . ,& -, .

& 5 6&/. ! -, . 6+ 0

5 0 . &, 0 , & . / 1 4

. . +6, 25 .. ( ), 6, 2 .. ( ), . &/+ 0,05 ..

( ). $638 . . -5 . & & . 6&/ 4 . ( ).

& + & ,& & 6 0, & / . 6

Special/Experimental Design/Create Design. ! 0 7 . 69

/ & ,& Mixture (.), 9 / + & & (1) & + ., (3).

& 9 , & 5 . , ., . 1 . . 4, / 9 33 1 33

5 6 , 5 9 + 4 .. & 638 -, , 5 ,& – . &. ' &3+ &/ 0 -,

0 , ,& (Simplex-Centroid – .,& 0

0 ,&) , & & 5 5 5 , . . ( . 4.15). ! 5 6,, , . & & 6 0 / Special Cubic

. 4.15. & 5 , . ,& , , & 3 ..

(, &/ 6 + . &/, & 3863 + . &/3

& . 7 5 , ., .). &,

54

69 6 . Augment Design (7 0 ,&) /

. Randomize.

. 4.16. + &/ ,& -, ..

! 6&/, . 0 , + &/ 63 6 ,& -, . ( . 4.16), 6 . ,&, 5 ,, , + . 4 ,0 1.

55

. 4.17. 6&/ & -, . &/ 01 01.

. 4.18. 6&/ & , &/ 6 + . &.

56

& -, . &/ 01 01 + 0 /

-& 63 & 6 , & / , , &/ 6 +, , 0

& 4.4.

' 7 38 -, 0 & -, . &/ 01

01. & -5 & 6 0, & / . 6 Special/Experimental Design/Analyze Design 0 7 . & 5 . &

, . 63 .

. 4.19. 6&/ 0 , 5 &.

! 6&/, 6&/ &

-, . &/ 01 01 ( . 4.17), 1 7 , +

+ + .0 -44 0 &3 3 6 +

(Quadratic) , &/ 6 + (Special Cubic) . & (p-Value < 0.05). &/ 6 , &/ 6 + . &/ & + ., /

&/ 7 & 6 . .

& 0 + , , &/ 6 + . & & 6 9 / , 6 & + 01 46 6 / . Model Results (6&/ 0 . &). $ , &6+ ( . 4.18) & 6, + +& 0 . &, . +& , . 3 + .0 -44 0

(p-Value < 0.05).

/ . & & . , 9 6&/ .

, 5 & ( . 4.19).

57

% 0 , &&3 / , &6+ 0 6&/, . 9

, &/ / 5 4 . , 1 & 6 0. 5 4 ., ., 9 , 6 5 4 + 1 46 , . ,6 0

Response Plot ( . 4.20).

. 4.20. 4 , 1 & 6 0 5 4 , 1 &.

5 4 , 1 & 1 7 0 . .6.

. .6. &, . 9 / , 0 7, , 01

5 . .6. .6& 4 .. & & + 5 , & -1 + & 6 , &/ / 0. 5 4..

$5 . 0 , & 6 -, . &/ 01 01 &

. . + .&/, , 0 38 .63 . / . 6& 4 . 5 5 ..

2 . &/ . & 638 :

E = 883,953 A + 798,862 B + 612,316 C + 5,63053 A B -

-907,46 A C - 1437,64 B C - 5527,04 A B C

5.0# % '(#+.

! . / , & &/ / ., 6, + 01

&6+ 0 . . 0 ..

58

! & + & &6+ 01 0, & . 01

0 , , & 9, + , & &/ 0 + 4 &

01 &3 3 + 0 , . 96 . (5

65 1 . 1 . 9 + , &3

.).

68 63 0 & & . 01 :

−, & , 0 ;

−, 5 (, 6 68 1 + . 5

, 8 . , 7&0. + .).

- & 63, + 0 . &/ 0& 4 , & & ., 4 . &/ ,. &/ . &/ , &, , & . 9 / , / . .0 0.

&/7 65 1 &, & . 01

, , & 5, + 0 9 (0+ &3+ 3863 &/ .,) (7 6), 0

6 69 56& 01 .,. &/7 .

& . 01 &3+ & + 0 , 0 4 &/ 76., , & 38 6 / 56& 63 & 3863 & + &.

&/7 56& 01 & 38 1 . 01

, & 9 6. & .: & 3 & , &

. , & 863 . + 63

& 63 & & 63 ., 6, . 9 . /

.. ! - - , + , 38 .,. - 56& 01 ., + , 6 63

..

5.1.# ! ' % '.

!, . 9 , . . &, , & 6 , 01 , 01 , , & + , ,. ! + 1 01 01 , &/ 63 9 . + 0 & , , 1995 5. , / 2004 5., , 0 & 5.1.

+ & . & . 5 1 . , & / -& 63 & 6 1 01 01. ! + & 0 +

&&/ + . , / .

(, ., ).

& ,6 & & 6 0, & / . 6 Special/Time-Series

Analysis/Descriptive Methods 0 7 . & 5 . 6 / + &/ 0 , . 0 & ( . 5.1), .: , & Data .

; 5 6,, Sampling Interval 6 / . , & 9 Month(s); , & Starting At / + &/ 63 6 – 1/95 (/

1995 5.). &/ 0 , & 69 / ..

59

& 5.1.

& 9 , , + &/ &

. 5 , 6 8 + & &3, + &

+ . & .

% 0 , &6+ / 5 4 + , &, & 6 9 /

, 6 5 4 + 1 46 0 / ,6 Horizontal Time Sequence Plot (5 &/ 0 5 4 . , & &/).

60